Optimized synthesis and characterization of La(OH)3 and LaB6 nanostructures for enhanced NIR optical filters

dc.contributor.authorBulbul, B. G.
dc.contributor.authorToprak, B. C.
dc.contributor.authorSayrac, M.
dc.contributor.authorOzen, Y.
dc.contributor.authorOzcelik, S
dc.date.accessioned2025-05-05T08:05:17Z
dc.date.available2025-05-05T08:05:17Z
dc.date.issued2024
dc.departmentFakülteler, Mühendislik Fakültesi, Nanoteknoloji Mühendisliği Bölümü
dc.description.abstractThe present study describes a method for synthesizing nanostructured La(OH)3 and LaB6 materials with efficient field emission properties using the spin coating technique. The study was motivated by the significant demand for the optical properties of LaB6 with efficient field emission properties using the spin coating technique in the near-infrared (NIR) region. The optimization of the LaB6 synthesis process for economic and reproducible results is highlighted, showcasing a systematic approach starting from La(OH)3 formation through chemical mixing and high-temperature heating, followed by boron incorporation. The systematic methodology includes forming La(OH)3 through chemical mixing and high-temperature heating, followed by combining it with boron to achieve the LaB6 structure. Characterization methods such as XRD, FTIR, SEM, AFM, and SIMS validated the successful synthesis and uniformity of the materials. Optical analyses showed increased visible transmittance and reduced infrared transmittance for the LaB6 thin film. Optical analyses showed increased visible transmittance and decreased infrared transmittance in the 110nmthick LaB6 film, with an absorption valley at 1000 nm. SEM images revealed microstructural features andAFManalysis indicated a homogeneous distribution of La and B atoms with anRMS value of 0.87 nm. SIMS analysis confirmed uniform atomic distribution throughout the film thickness. The optimized recipes contribute to the efficiency and controllability of the synthesis process. The presented results provide valuable insights into material synthesis methodologies and serve as a crucial reference for utilizing LaB6 materials in infrared devices.
dc.identifier.citationB G Bulbul, B C Toprak, M Sayrac, Y Ozen and S Ozcelik Physica Scripta, Volume 99, Number 11 2024
dc.identifier.doi10.1088/1402-4896/ad7db9
dc.identifier.endpage13
dc.identifier.issue115913
dc.identifier.scopusqualityQ2
dc.identifier.startpage1
dc.identifier.urihttps://hdl.handle.net/20.500.12418/35691
dc.identifier.volume99
dc.identifier.wosqualityQ2
dc.indekslendigikaynakWeb of Science
dc.institutionauthorSayrac, M.
dc.institutionauthoridhttps://orcid.org/0000-0003-4373-6897
dc.language.isoen
dc.publisherIOP Publishing
dc.relation.ispartofPhysica Scripta
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/openAccess
dc.titleOptimized synthesis and characterization of La(OH)3 and LaB6 nanostructures for enhanced NIR optical filters
dc.typeArticle

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