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dc.contributor.authorAltunay, Nail
dc.contributor.authorElik, Adil
dc.contributor.authorGurkan, Ramazan
dc.date.accessioned2019-07-27T12:10:23Z
dc.date.accessioned2019-07-28T09:37:00Z
dc.date.available2019-07-27T12:10:23Z
dc.date.available2019-07-28T09:37:00Z
dc.date.issued2019
dc.identifier.issn1936-9751
dc.identifier.issn1936-976X
dc.identifier.urihttps://dx.doi.org/10.1007/s12161-019-01514-7
dc.identifier.urihttps://hdl.handle.net/20.500.12418/5854
dc.descriptionWOS: 000473176500006en_US
dc.description.abstractIn this study, a practical and rapid microextraction procedure based on ionic liquid (IL) was proposed for the spectrophotometric determination of morin (2-(2,4-dihydroxyphenyl)-3,5,7-trihydroxychromen-4-one) in foods and beverages. The extraction of morin from the sample matrix was carried out as follows. Firstly, a chelate complex of the morin with Ni(II) was formed in presence of citrate buffer of pH 5.5. Then, 1-hexyl-3-methylimidazolium bis(trifluoromethylsulfonyl)imide, [C(6)mim] [Tf2N], as extracting IL was added to the sample solution. The complex formed was attached to the microspheres of the [C(6)mim] [Tf2N] using vortex, finally separated and extracted from aqueous medium by centrifugation. The main variables affecting extraction efficiency were investigated and optimized. Under optimized conditions, the proposed method exhibits a linear working range of 17.5-550 mu g L-1 with a sensitivity enhancement of 126-fold. Furthermore, the detection limit, relative standard deviations (RSD%, n 5), and total extraction time were 5.3 mu g L-1, 1.9%, and 8 min with a recovery ranging from 91.8 to 103.6%, respectively. Following the repeatability and reproducibility studies, the method was successfully applied to the trace analysis of morin in various food and beverages.en_US
dc.language.isoengen_US
dc.publisherSPRINGERen_US
dc.relation.isversionof10.1007/s12161-019-01514-7en_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectMorinen_US
dc.subjectExtractionen_US
dc.subjectSpectrophotometryen_US
dc.subjectAntioxidanten_US
dc.subjectFoodsen_US
dc.subjectBeveragesen_US
dc.titleA Simple and Green Microextraction Procedure for Extraction of Morin in Food and Beverages Using Ionic Liquiden_US
dc.typearticleen_US
dc.relation.journalFOOD ANALYTICAL METHODSen_US
dc.contributor.department[Altunay, Nail -- Elik, Adil -- Gurkan, Ramazan] Cumhuriyet Univ, Dept Chem, Fac Sci, TR-58140 Sivas, Turkeyen_US
dc.identifier.volume12en_US
dc.identifier.issue8en_US
dc.identifier.endpage1758en_US
dc.identifier.startpage1747en_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US


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