dc.contributor.author | Akkurt, Mehmet | |
dc.contributor.author | Celik, Ismail | |
dc.contributor.author | Demir, Hale | |
dc.contributor.author | Ozkirimli, Sumru | |
dc.contributor.author | Buyukgungor, Orhan | |
dc.date.accessioned | 2019-07-27T12:10:23Z | |
dc.date.accessioned | 2019-07-28T10:06:01Z | |
dc.date.available | 2019-07-27T12:10:23Z | |
dc.date.available | 2019-07-28T10:06:01Z | |
dc.date.issued | 2011 | |
dc.identifier.issn | 1600-5368 | |
dc.identifier.uri | https://dx.doi.org/10.1107/S1600536811000481 | |
dc.identifier.uri | https://hdl.handle.net/20.500.12418/9609 | |
dc.description | WOS: 000287034000178 | en_US |
dc.description | PubMed ID: 21522985 | en_US |
dc.description.abstract | In the title compound, C16H14N4O4S center dot H2O, the benzene and pyridine rings make a dihedral angle of 85.8 (1)degrees. Both enantiomers of the chiral title compound are statistically disordered over the same position in the unit cell. The methyl and carbonyl group attached to the stereogenic center (C-5 of the thiazolidine ring) were therefore refined with common site-occupation factors of 0.531 (9) and 0.469 (9), respectively, for each stereoisomer. In the crystal, intermolecular N-H center dot center dot center dot O, O-H center dot center dot center dot O and O-H center dot center dot center dot N hydrogen bonds link the molecules, forming a three-dimensional supramolecular network. The crystal structure further shows pi-pi stacking interactions [centroid-centroid distance = 3.5063 (13) angstrom] between the pyridine rings. | en_US |
dc.description.sponsorship | University Research Fund [F.279] | en_US |
dc.description.sponsorship | The authors acknowledge the Faculty of Arts and Sciences, Ondokuz Mayis University, Turkey, for the use of the Stoe IPDS 2 diffractometer (purchased under grant F.279 of the University Research Fund). HD and SO acknowledge the Scientific Research Projects Coordination Unit of Istanbul University (Project number T-3691). | en_US |
dc.language.iso | eng | en_US |
dc.publisher | WILEY-BLACKWELL | en_US |
dc.relation.isversionof | 10.1107/S1600536811000481 | en_US |
dc.rights | info:eu-repo/semantics/openAccess | en_US |
dc.title | N-[5-Methyl-2-(2-nitrophenyl)-4-oxo-1,3-thiazolidin-3-yl]pyridine-3-carboxamide monohydrate | en_US |
dc.type | article | en_US |
dc.relation.journal | ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | en_US |
dc.contributor.department | [Akkurt, Mehmet] Erciyes Univ, Dept Phys, Fac Sci, TR-38039 Kayseri, Turkey -- [Celik, Ismail] Cumhuriyet Univ, Fac Arts & Sci, Dept Phys, TR-58140 Sivas, Turkey -- [Demir, Hale -- Ozkirimli, Sumru] Istanbul Univ, Dept Pharmaceut Chem, Fac Pharm, TR-34116 Istanbul, Turkey -- [Buyukgungor, Orhan] Ondokuz Mayis Univ, Fac Arts & Sci, Dept Phys, TR-55139 Samsun, Turkey | en_US |
dc.identifier.volume | 67 | en_US |
dc.identifier.endpage | U2204 | en_US |
dc.identifier.startpage | O293 | en_US |
dc.relation.publicationcategory | Makale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı | en_US |