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dc.contributor.authorAkkurt, Mehmet
dc.contributor.authorCelik, Ismail
dc.contributor.authorDemir, Hale
dc.contributor.authorOzkirimli, Sumru
dc.contributor.authorBuyukgungor, Orhan
dc.date.accessioned2019-07-27T12:10:23Z
dc.date.accessioned2019-07-28T10:06:01Z
dc.date.available2019-07-27T12:10:23Z
dc.date.available2019-07-28T10:06:01Z
dc.date.issued2011
dc.identifier.issn1600-5368
dc.identifier.urihttps://dx.doi.org/10.1107/S1600536811000481
dc.identifier.urihttps://hdl.handle.net/20.500.12418/9609
dc.descriptionWOS: 000287034000178en_US
dc.descriptionPubMed ID: 21522985en_US
dc.description.abstractIn the title compound, C16H14N4O4S center dot H2O, the benzene and pyridine rings make a dihedral angle of 85.8 (1)degrees. Both enantiomers of the chiral title compound are statistically disordered over the same position in the unit cell. The methyl and carbonyl group attached to the stereogenic center (C-5 of the thiazolidine ring) were therefore refined with common site-occupation factors of 0.531 (9) and 0.469 (9), respectively, for each stereoisomer. In the crystal, intermolecular N-H center dot center dot center dot O, O-H center dot center dot center dot O and O-H center dot center dot center dot N hydrogen bonds link the molecules, forming a three-dimensional supramolecular network. The crystal structure further shows pi-pi stacking interactions [centroid-centroid distance = 3.5063 (13) angstrom] between the pyridine rings.en_US
dc.description.sponsorshipUniversity Research Fund [F.279]en_US
dc.description.sponsorshipThe authors acknowledge the Faculty of Arts and Sciences, Ondokuz Mayis University, Turkey, for the use of the Stoe IPDS 2 diffractometer (purchased under grant F.279 of the University Research Fund). HD and SO acknowledge the Scientific Research Projects Coordination Unit of Istanbul University (Project number T-3691).en_US
dc.language.isoengen_US
dc.publisherWILEY-BLACKWELLen_US
dc.relation.isversionof10.1107/S1600536811000481en_US
dc.rightsinfo:eu-repo/semantics/openAccessen_US
dc.titleN-[5-Methyl-2-(2-nitrophenyl)-4-oxo-1,3-thiazolidin-3-yl]pyridine-3-carboxamide monohydrateen_US
dc.typearticleen_US
dc.relation.journalACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINEen_US
dc.contributor.department[Akkurt, Mehmet] Erciyes Univ, Dept Phys, Fac Sci, TR-38039 Kayseri, Turkey -- [Celik, Ismail] Cumhuriyet Univ, Fac Arts & Sci, Dept Phys, TR-58140 Sivas, Turkey -- [Demir, Hale -- Ozkirimli, Sumru] Istanbul Univ, Dept Pharmaceut Chem, Fac Pharm, TR-34116 Istanbul, Turkey -- [Buyukgungor, Orhan] Ondokuz Mayis Univ, Fac Arts & Sci, Dept Phys, TR-55139 Samsun, Turkeyen_US
dc.identifier.volume67en_US
dc.identifier.endpageU2204en_US
dc.identifier.startpageO293en_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US


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