| dc.contributor.author | Hazer, Baki | |
| dc.contributor.author | Elik Adil | |
| dc.contributor.author | Tüzen, Mustafa | |
| dc.contributor.author | Altunay Nail | |
| dc.date.accessioned | 2023-04-12T07:27:58Z | |
| dc.date.available | 2023-04-12T07:27:58Z | |
| dc.date.issued | 2022 | tr |
| dc.identifier.citation | Mustafa Tuzen a,b
, Baki Hazer c,d
, Adil Elik e
, Nail Altunay e,*
a Department of Chemistry, Tokat Gaziosmanpasa University, Tokat, Turkey b King Fahd University of Petroleum and Minerals, Research Institute, Center for Environment and Marine Studies, Dhahran, 31261 Saudi Arabia c Department of Aircraft Airframe Engine Maintenance, Kapadokya University, Nevs¸ehir, Turkey d Zonguldak Bülent Ecevit University, Department of Chemistry, 67100 Zonguldak, Turkey e Department of Chemistry, Sivas Cumhuriyet University, Sivas, Turkey | tr |
| dc.identifier.uri | https://hdl.handle.net/20.500.12418/13620 | |
| dc.description.abstract | A new and novel poly(vinyl benzyl dithiocarbonate-dimethyl amino ethyl methacrylate) block copolymer (Pvb-DMA-Xa) as adsorbent was synthesized for the vortex-assisted dispersive solid phase microextraction (VA-DSPME) of patulin from apple products and dried fruits using Uv–visible spectrophotometer. The characterization of synthesized Pvb-DMA-Xa block copolymer was performed with Fourier Transform Infrared spectroscopy (FTIR-ATR) technique. Analytical characteristics such as pH, sorbent amount, adsorption time, eluent type and its volume, desorption time and adsorption capacity were optimized. Limit of detection (3Sb/m) and limit of quantitation (10Sb/m) were found 0.3 and 1.0 ng mL−1. Linear dynamic range (LDR), relative standard deviation (RSD) and recovery values were found in the range of 1–30 ng mL−1, 2.1–2.7 % and 93.5–97.3 %, respectively. Enhancement factor (EF) was found 193. The accuracy of the method was confirmed with standard addition method and analyzing of samples by reference method. | tr |
| dc.language.iso | eng | tr |
| dc.rights | info:eu-repo/semantics/closedAccess | tr |
| dc.subject | Patulin Apple products Dried fruits Dispersive solid phase microextraction UV–VIS spectrophotometer Poly(vinyl benzyl dithiocarbonate-dimethyl amino ethyl methacrylate) block copolymer | tr |
| dc.title | Synthesized of poly(vinyl benzyl dithiocarbonate-dimethyl amino ethyl methacrylate) block copolymer as adsorbent for the vortex-assisted dispersive solid phase microextraction of patulin from apple products and dried fruits | tr |
| dc.type | article | tr |
| dc.contributor.department | Fen Fakültesi | tr |
| dc.relation.publicationcategory | Uluslararası Hakemli Dergide Makale - Kurum Öğretim Elemanı | tr |
