dc.contributor.author | Celik, Ismail | |
dc.contributor.author | Akkurt, Mehmet | |
dc.contributor.author | Jarrahpour, Aliasghar | |
dc.contributor.author | Rad, Javad Ameri | |
dc.contributor.author | Celik, Omer | |
dc.date.accessioned | 2019-07-27T12:10:23Z | |
dc.date.accessioned | 2019-07-28T09:56:18Z | |
dc.date.available | 2019-07-27T12:10:23Z | |
dc.date.available | 2019-07-28T09:56:18Z | |
dc.date.issued | 2015 | |
dc.identifier.issn | 2056-9890 | |
dc.identifier.uri | https://dx.doi.org/10.1107/S2056989015002959 | |
dc.identifier.uri | https://hdl.handle.net/20.500.12418/7942 | |
dc.description | WOS: 000369973400038 | en_US |
dc.description | PubMed ID: 25844239 | en_US |
dc.description.abstract | The central beta-lactam ring of the title compound, C36H24N2O4, is almost planar (r.m.s. deviation = 0.003 angstrom) and makes dihedral angles of 17.17 (19), 89.76 (17) and 78.44 (17)degrees with the benzene ring, the anthracene ring (r.m.s. deviation = 0.003 angstrom) and the 1H-benzo[de] isoquinoline-1,3(2H)-dione moiety, which is nearly planar [maximum deviation = 0.098 (2) angstrom], respectively. The molecular structure is stabilized by an intramolecular C-H center dot center dot center dot N hydrogen bond. In the crystal, molecules are linked via C-H center dot center dot center dot pi and pi-pi stacking interactions [centroid-centroid distances = 3.5270 (19) and 3.779 (2) angstrom], forming a three-dimensional structure. A region of disordered electron density, probably disordered solvent molecules, was treated with the SQUEEZE procedure in PLATON [Spek (2015). Acta Cryst. C71, 9-18], which indicated a solvent cavity of 322 angstrom(3) containing approximately 91 electrons. Their formula mass and unit-cell characteristics were not taken into account during the refinement. | en_US |
dc.language.iso | eng | en_US |
dc.publisher | INT UNION CRYSTALLOGRAPHY | en_US |
dc.relation.isversionof | 10.1107/S2056989015002959 | en_US |
dc.rights | info:eu-repo/semantics/openAccess | en_US |
dc.subject | crystal structure | en_US |
dc.subject | beta-lactam ring | en_US |
dc.subject | 2-azetidinone | en_US |
dc.subject | anthracene | en_US |
dc.subject | intramolecular C-H center dot center dot center dot N hydrogen bond | en_US |
dc.subject | C-H center dot center dot center dot pi interactions | en_US |
dc.subject | pi-pi stacking interactions | en_US |
dc.title | Crystal structure of 2-[(3S, 4S)-4-(anthracen-9-yl)-1-(4-methoxyphenyl)-2-oxoazetidin-3-yl]-2-aza-2H-phenalene-1,3-dione unknown solvate | en_US |
dc.type | article | en_US |
dc.relation.journal | ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | en_US |
dc.contributor.department | [Celik, Ismail] Cumhuriyet Univ, Fac Arts & Sci, Dept Phys, TR-06532 Sivas, Turkey -- [Akkurt, Mehmet] Erciyes Univ, Fac Sci, Dept Phys, TR-38039 Kayseri, Turkey -- [Jarrahpour, Aliasghar -- Rad, Javad Ameri] Shiraz Univ, Coll Sci, Dept Chem, Shiraz 71454, Iran -- [Celik, Omer] Dicle Univ, Dept Phys, Fac Educ, TR-21280 Diyarbakir, Turkey -- [Celik, Omer] Dicle Univ, Sci & Technol Applicat & Res Ctr, TR-21280 Diyarbakir, Turkey | en_US |
dc.contributor.authorID | Celik, Omer -- 0000-0002-3314-6132 | en_US |
dc.identifier.volume | 71 | en_US |
dc.identifier.endpage | + | en_US |
dc.identifier.startpage | O184 | en_US |
dc.relation.publicationcategory | Makale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı | en_US |