Highly Simple Deep Eutectic Solvent Extraction of Manganese in Vegetable Samples Prior to Its ICP-OES Analysis

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dc.authoridSoylak, Mustafa -- 0000-0002-1017-0244en_US
dc.contributor.authorBagda, Esra
dc.contributor.authorAltundag, Huseyin
dc.contributor.authorSoylak, Mustafa
dc.date.accessioned2019-07-27T12:10:23Z
dc.date.accessioned2019-07-28T09:40:17Z
dc.date.available2019-07-27T12:10:23Z
dc.date.available2019-07-28T09:40:17Z
dc.date.issued2017
dc.department[Bagda, Esra] Cumhuriyet Univ, Fac Pharm, TR-58140 Sivas, Turkey -- [Altundag, Huseyin] Sakarya Univ, Dept Chem, Fac Sci & Arts, TR-54187 Adapazari, Sakarya, Turkey -- [Soylak, Mustafa] Erciyes Univ, Dept Chem, Fac Sci, TR-38039 Kayseri, Turkeyen_US
dc.description.abstractIn the present work, simple and sensitive extraction methods for selective determination of manganese have been successfully developed. The methods were based on solubilization of manganese in deep eutectic solvent medium. Three deep eutectic solvents with choline chloride (vitamin B4) and tartaric/oxalic/citric acids have been prepared. Extraction parameters were optimized with using standard reference material (1573a tomato leaves). The quantitative recovery values were obtained with 1.25 g/L sample to deep eutectic solvent (DES) volume, at 95 A degrees C for 2 h. The limit of detection was found as 0.50, 0.34, and 1.23 mu g/L for DES/tartaric, DES/oxalic, and DES/citric acid, respectively. At optimum conditions, the analytical signal was linear for the range of 10-3000 mu g/L for all studied DESs with the correlation coefficient > 0.99. The extraction methods were applied to different real samples such as basil herb, spinach, dill, and cucumber barks. The known amount of manganese was spiked to samples, and good recovery results were obtained.en_US
dc.description.sponsorshipUnit of the Scientific Research Projects of Cumhuriyet University; Cumhuriyet Cumhuriyet University Advanced Technology Research Center (CUTAM); Unit of the Scientific Research Projects of Sakarya University; Erciyes Universityen_US
dc.description.sponsorshipThe authors are fully grateful for the financial support of the Unit of the Scientific Research Projects of Cumhuriyet University, Cumhuriyet Cumhuriyet University Advanced Technology Research Center (CUTAM), Unit of the Scientific Research Projects of Sakarya University, and Erciyes University.en_US
dc.identifier.doi10.1007/s12011-017-0967-5en_US
dc.identifier.endpage339en_US
dc.identifier.issn0163-4984
dc.identifier.issn1559-0720
dc.identifier.issue2en_US
dc.identifier.pmid28233088en_US
dc.identifier.scopus2-s2.0-85013654703en_US
dc.identifier.scopusqualityQ1
dc.identifier.startpage334en_US
dc.identifier.urihttps://dx.doi.org/10.1007/s12011-017-0967-5
dc.identifier.urihttps://hdl.handle.net/20.500.12418/6655
dc.identifier.volume179en_US
dc.identifier.wosWOS:000410023900020en_US
dc.identifier.wosqualityQ3
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.indekslendigikaynakPubMeden_US
dc.language.isoenen_US
dc.publisherHUMANA PRESS INCen_US
dc.relation.ispartofBIOLOGICAL TRACE ELEMENT RESEARCHen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectDeep eutectic solvent extractionen_US
dc.subjectManganeseen_US
dc.subjectVegetable samplesen_US
dc.titleHighly Simple Deep Eutectic Solvent Extraction of Manganese in Vegetable Samples Prior to Its ICP-OES Analysisen_US
dc.typeArticleen_US

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