Investigation of vortex assisted magnetic deep eutectic solvent based dispersive liquid-liquid microextraction for separation and determination of vanadium from water and food matrices: Multivariate analysis

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dc.authoridTuzen, Mustafa/0000-0001-8522-6620
dc.contributor.authorAltunay, Nail
dc.contributor.authorLanjwani, Muhammad Farooque
dc.contributor.authorTuzen, Mustafa
dc.contributor.authorBoczkaj, Grzegorz
dc.date.accessioned2024-10-26T18:09:51Z
dc.date.available2024-10-26T18:09:51Z
dc.date.issued2024
dc.departmentSivas Cumhuriyet Üniversitesi
dc.description.abstractA new and simple vortex assisted magnetic deep eutectic solvent dispersive liquid-liquid microextraction procedure (VA-MDES-DLLME) was developed for the determination of vanadium (V) in food and water samples by flame atomic absorption spectrometry (FAAS). In the extraction medium, a bis(acetylpivalylmethane) ethylenediimine (H2APM2en) was used for the complexation of V(V) in sample solution at pH 6. The VA-MDESDLLME was optimized by different operation parameters, pH level of solution, MDESs volume, vortex time, concentration of complexing agent and samples volume. The accuracy of VA-MDES-DLLME was confirmed by analysis of certified reference materials (CRMs) and standard additional method in respect to real samples. The detection limit, quantification limit and enhancement factor were found 0.3, 1.0 ng mL-1 and 120, respectively. The linearity was confirmed for wide concentration range from 1 to 600 ng mL-1 and relative standard deviation (RSD) is 2.8 %. The multivariate statistical analysis was used for factorial design to explore the effects of extraction parameters on recovery of V(V) and also significant level of variables.
dc.description.sponsorshipTurkiye Burslary; TUBA
dc.description.sponsorshipM.F Lanjwani thanks to Turkiye Burslary for its supports. Dr. M. Tuzen thanks to TUBA for partly supports.
dc.identifier.doi10.1016/j.molliq.2024.124000
dc.identifier.issn0167-7322
dc.identifier.issn1873-3166
dc.identifier.scopus2-s2.0-85182598772
dc.identifier.scopusqualityQ1
dc.identifier.urihttps://doi.org/10.1016/j.molliq.2024.124000
dc.identifier.urihttps://hdl.handle.net/20.500.12418/30304
dc.identifier.volume396
dc.identifier.wosWOS:001166503900001
dc.identifier.wosqualityN/A
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoen
dc.publisherElsevier
dc.relation.ispartofJournal of Molecular Liquids
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.subjectVortex assisted magnetic deep eutectic solvent
dc.subjectDispersiveliquid-liquid microextraction
dc.subjectVanadium
dc.subjectWater and food samples
dc.subjectAtomic absorption spectrometry
dc.subjectMultivariate statistical analysis
dc.titleInvestigation of vortex assisted magnetic deep eutectic solvent based dispersive liquid-liquid microextraction for separation and determination of vanadium from water and food matrices: Multivariate analysis
dc.typeArticle

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