Deep Eutectic Solvent-based Extraction of As, Mn, Pb, Cr, and Ni from Spleen, Kidney, and Brain Samples
| dc.contributor.author | Bağda, Esra | |
| dc.contributor.author | Altundağ, Hüseyin | |
| dc.contributor.author | Keskin, Can Serkan | |
| dc.date.accessioned | 2023-06-22T13:37:02Z | |
| dc.date.available | 2023-06-22T13:37:02Z | |
| dc.date.issued | 14 September 2022 | tr |
| dc.department | Eğitim Bilimleri Enstitüsü | tr |
| dc.description.abstract | Deep eutectic solvent extraction for As, Mn, Pb, Cr, and Ni from spleen, kidney, and brain samples was investigated. The experimental parameters such as type and amount of deep eutectic solvent and sample/deep eutectic solvent ratio were optimized. The method optimization was conducted with the certified reference material (BCR 185-R). The analytical characteristics such as limits of detection and quantitation, relative standard deviation, and calibration equations were determined. Different deep eutectic solvent types were prepared and examined for better extraction. Choline chloride was used as a quaternary ammonium salt, and oxalic acid, urea, thiourea, and citric acid were used as hydrogen bond donors. Better results and recoveries higher than 90% were obtained with oxalic acid. The calculated LOD values for As, Mn, Pb, Cr, and Ni were 1.1, 0.3, 1.3, 1.4, 0.8, and LOQ values were 3.8, 1.1, 4.3, 4.7, 2.7 mg/kg, respectively. | tr |
| dc.identifier.citation | Esra Bağdaa, *, Hüseyin Altundağb , and Can Serkan Keskinb a Department of Basic Pharmaceutical Sciences, Analytical Chemistry Division, Faculty of Pharmacy, Sivas Cumhuriyet University, Sivas, 58140 Turkey b Department of Chemistry, Analytical Chemistry Division, Faculty of Art and Science, Sakarya University, Sakarya, 54050 Turkey *e-mail: esraer@cumhuriyet.edu.tr Received August 25, 2020; revised March 2, 2022; accepted March 10, 2022 | tr |
| dc.identifier.scopus | 2-s2.0-85138017023 | en_US |
| dc.identifier.scopusquality | N/A | |
| dc.identifier.uri | https://hdl.handle.net/20.500.12418/13988 | |
| dc.identifier.wos | WOS:000853858800004 | en_US |
| dc.identifier.wosquality | Q4 | |
| dc.indekslendigikaynak | Web of Science | en_US |
| dc.indekslendigikaynak | Scopus | en_US |
| dc.language.iso | en | en_US |
| dc.relation.publicationcategory | Uluslararası Hakemli Dergide Makale - Kurum Öğretim Elemanı | tr |
| dc.rights | info:eu-repo/semantics/embargoedAccess | tr |
| dc.subject | deep eutectic solvent, spleen, kidney, brain, extraction | tr |
| dc.title | Deep Eutectic Solvent-based Extraction of As, Mn, Pb, Cr, and Ni from Spleen, Kidney, and Brain Samples | en_US |
| dc.type | Article | en_US |
