Air-Assisted Alkanol-Based Nanostructured Supramolecular Liquid-Liquid Microextraction for Extraction and Spectrophotometric Determination of Morin in Fruit and Beverage Samples

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dc.authoridAfshar mogaddam, Mohammad reza/0000-0003-1144-4523
dc.contributor.authorDemir, Ozge
dc.contributor.authorTuzen, Mustafa
dc.contributor.authorAltunay, Nail
dc.contributor.authorMogaddam, Mohammad Reza Afshar
dc.date.accessioned2024-10-26T18:09:25Z
dc.date.available2024-10-26T18:09:25Z
dc.date.issued2022
dc.departmentSivas Cumhuriyet Üniversitesi
dc.description.abstractA new air-assisted liquid-liquid microextraction method based on alkanol nanostructured supramolecular solvents coupled to spectrometric analysis was developed for extraction, preconcentration, and spectrophotometric determination of morin. Al(III)-morin complex was performed at pH 4.5. Four different alkanol-based SUPRAS (supramolecular solvents) were prepared for the separation and preconcentration of Al-morin complex from aqueous solution by using vortex and centrifugation. Effect of analytical variables and tolerance limit of matrix ions were investigated. Under the optimum conditions, detection limit, quantification limit, relative standard deviation, preconcentration factor, and enhancement factor were found as 3.5 mu g L-1, 10 mu g L-1, 3.1%, 120, and 95, respectively. The accuracy of the method was performed with standard addition. The obtained results demonstrated the applicability of the method for the separation, preconcentration, and determination of morin in fruit and beverage samples. The method also complies with green chemistry principles as it uses green solvents, reduces reagent volumes, and produces low amounts of waste.
dc.identifier.doi10.1007/s12161-021-02111-3
dc.identifier.endpage251
dc.identifier.issn1936-9751
dc.identifier.issn1936-976X
dc.identifier.issue1
dc.identifier.pmid34484555
dc.identifier.scopus2-s2.0-85114037208
dc.identifier.scopusqualityQ2
dc.identifier.startpage243
dc.identifier.urihttps://doi.org/10.1007/s12161-021-02111-3
dc.identifier.urihttps://hdl.handle.net/20.500.12418/30078
dc.identifier.volume15
dc.identifier.wosWOS:000691926600001
dc.identifier.wosqualityQ2
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.indekslendigikaynakPubMed
dc.language.isoen
dc.publisherSpringer
dc.relation.ispartofFood Analytical Methods
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/openAccess
dc.subjectAir-assisted alkanol-based microextraction
dc.subjectSupramolecular solvent
dc.subjectLiquid-liquid microextraction
dc.subjectMorin
dc.subjectFruit
dc.subjectBeverage
dc.titleAir-Assisted Alkanol-Based Nanostructured Supramolecular Liquid-Liquid Microextraction for Extraction and Spectrophotometric Determination of Morin in Fruit and Beverage Samples
dc.typeArticle

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