Optimization of a rapid and sensitive ultrasound-assisted liquid-liquid microextraction using switchable hydrophilicity solvent for extraction of ?-carotene in fruit juices and vegetables

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dc.contributor.authorAltunay, Nail
dc.contributor.authorTuzen, Mustafa
dc.contributor.authorLanjwani, Muhammad Farooque
dc.contributor.authorReza, Mohammad
dc.contributor.authorMogaddam, Afshar
dc.date.accessioned2024-10-26T18:09:50Z
dc.date.available2024-10-26T18:09:50Z
dc.date.issued2022
dc.departmentSivas Cumhuriyet Üniversitesi
dc.description.abstractA simple, rapid and sensitive ultrasound-assisted liquid-liquid microextraction by switchable hydrophilicity solvent (UA-LLME-SHS) method was developed first time for extraction and determination of beta-carotene from fruit juices and vegetables using a spectrophotometer. The effect of pH, solvent dose, ultrasound time, volume of NH4OH, volume of NaCl (w/v) and effects of different chemicals on extraction recovery was investigated. The proposed method showed good extraction recovery of beta-carotene. The working range of the developed method was 50-700 ng mL(-1). Limits of detection and quantification were 15.5 mu g L(-1 )and 50 mu g L-1, respectively. The intraday and interday precisions of the developed method was investigated for 75 ng mL(-1) and 400 ng mL(-1) of p-carotene. As a result of the study, the relative standard deviation values were in the range of 2.8-3.3 % and 3.0-4.2 % for the intraday and interday studies, respectively. The enhancement factor was 114 and extraction recovery of beta-carotene was found 98.3 %. The factorial design was drawn to know the combined effects of variables and their significant and insignificant effects on the determination of the beta-carotene.
dc.description.sponsorshipTurkish Academy of Sciences (TUBA), Turkey; Turkey Bursary
dc.description.sponsorshipMuhammad Farooque Lanjwani thanks to Turkey Bursary for his financial supports. Dr. Mustafa Tuzen also thanks to Turkish Academy of Sciences (TUBA), Turkey for partial supports.
dc.identifier.doi10.1016/j.jfca.2022.104791
dc.identifier.issn0889-1575
dc.identifier.issn1096-0481
dc.identifier.scopus2-s2.0-85135418883
dc.identifier.scopusqualityQ1
dc.identifier.urihttps://doi.org/10.1016/j.jfca.2022.104791
dc.identifier.urihttps://hdl.handle.net/20.500.12418/30274
dc.identifier.volume114
dc.identifier.wosWOS:000888570400005
dc.identifier.wosqualityQ2
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoen
dc.publisherAcademic Press Inc Elsevier Science
dc.relation.ispartofJournal of Food Composition and Analysis
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.subjectbeta-carotene
dc.subjectReal samples
dc.subjectMicroextraction
dc.subjectSwitchable
dc.subjectSpectrophotometer
dc.subjectFactorial design
dc.titleOptimization of a rapid and sensitive ultrasound-assisted liquid-liquid microextraction using switchable hydrophilicity solvent for extraction of ?-carotene in fruit juices and vegetables
dc.typeArticle

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