Determination of zirconium in water, dental materials and artificial saliva after surfactant assisted dispersive ionic liquid based microextraction

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dc.contributor.authorBagda, Esra
dc.contributor.authorTuzen, Mustafa
dc.date.accessioned2019-07-27T12:10:23Z
dc.date.accessioned2019-07-28T09:56:25Z
dc.date.available2019-07-27T12:10:23Z
dc.date.available2019-07-28T09:56:25Z
dc.date.issued2015
dc.department[Bagda, Esra] Cumhuriyet Univ, Fac Pharm, TR-58140 Sivas, Turkey -- [Tuzen, Mustafa] Gaziosmanpasa Univ, Dept Chem, Fac Sci & Arts, TR-60250 Tokat, Turkeyen_US
dc.description.abstractIn this study, an extractive spectrophotometric method is proposed for the determination of trace amounts of zirconium. The method is based on the complex formation between zirconium and 2-(5-bromo-2-pyridylazo)-5-(diethylamino) phenol. Then, the formed complex is concentrated in an ionic liquid (1-hexyl-3-methylimidazolium hexafluorophosphate) phase. The parameters were optimized and analytical figures of merit were obtained. The tolerance limits for diverse ions were calculated. The enhancement factor (EF) and limit of detection (LOD) were found to be 156 and 0.012 mu g L-1, respectively. The relative standard deviation (RSD) was found to be lower than 6%. The proposed method has been successfully applied to water and environmental materials.en_US
dc.description.sponsorshipUnit of the Scientific Research Project of Cumhuriyet University; Unit of the Scientific Research Project of Gaziosmanpasa University; Turkish Academy of Sciencesen_US
dc.description.sponsorshipThe authors are fully grateful for the financial support of the Unit of the Scientific Research Projects of Cumhuriyet University and Gaziosmanpasa University. Dr. Mustafa Tuzen thanks to Turkish Academy of Sciences for financial support. The authors also thank to Assoc. Prof. Dr. Derya Ozdemir Dogan for providing the dental filling materials.en_US
dc.identifier.doi10.1039/c5ra21267gen_US
dc.identifier.endpage107879en_US
dc.identifier.issn2046-2069
dc.identifier.issue130en_US
dc.identifier.scopus2-s2.0-84952333982en_US
dc.identifier.scopusqualityQ2
dc.identifier.startpage107872en_US
dc.identifier.urihttps://dx.doi.org/10.1039/c5ra21267g
dc.identifier.urihttps://hdl.handle.net/20.500.12418/8000
dc.identifier.volume5en_US
dc.identifier.wosWOS:000367271700076en_US
dc.identifier.wosqualityQ2
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.language.isoenen_US
dc.publisherROYAL SOC CHEMISTRYen_US
dc.relation.ispartofRSC ADVANCESen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.titleDetermination of zirconium in water, dental materials and artificial saliva after surfactant assisted dispersive ionic liquid based microextractionen_US
dc.typeArticleen_US

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