Ultrasound-assisted dispersive micro solid phase extraction of maneb in water and food samples with new hybrid block copolymer material prior to micro-spectrophotometric analysis

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dc.contributor.authorAltunay, Nail
dc.contributor.authorHazer, Baki
dc.contributor.authorLanjwani, Muhammad Farooque
dc.contributor.authorTuzen, Mustafa
dc.date.accessioned2024-10-26T18:09:58Z
dc.date.available2024-10-26T18:09:58Z
dc.date.issued2025
dc.departmentSivas Cumhuriyet Üniversitesi
dc.description.abstractA simple and effective ultrasound-assisted dispersive micro solid-phase extraction (UA-d mu SPE) method was developed for the spectrophotometric determination of traces maneb in food and water. In this study, a new hybrid block copolymer poly (vinyl benzyl chloride-b-dimethyl aminoethyl methacrylate) (Pvb-DMA) was synthesized and characterized using techniques such as FTIR, SEM-EDX. The synthesized Pvb-DMA was used as an adsorbent for the extraction of maneb for first time in this study. The effects of different experimental variables such as pH, adsorbent amount, sample volume, eluent type were optimized. The statistical toll factorial design was applied to estimate the individual and combined impact of parameters on the extraction of maneb. The applicability of different solvents such as acetone, methanol, ethanol, tetrahydrofuran, acetonitrile for maneb recovery from adsorbent was tested. The detection and quantification limits were found to be 3.3 ng mL(-1) and 10.0 ng mL(-1), respectively. In addition, the preconcentration factor and linear range was obtained 300 and 10-500 ng mL(-1). The extraction recovery and relative standard deviation were found to be 95 % and 2.8 %, respectively.
dc.description.sponsorshipKapadokya University [KUN.2023-BAGP-020]; TUBA
dc.description.sponsorshipProfessor Dr. Baki Hazer thanks to Kapadokya University (KUN.2023-BAGP-020) for financial support. Professor Dr. Mustafa Tuzen thanks to TUBA for partial supports.
dc.identifier.doi10.1016/j.foodchem.2024.141098
dc.identifier.issn0308-8146
dc.identifier.issn1873-7072
dc.identifier.pmid39265405
dc.identifier.scopus2-s2.0-85203547790
dc.identifier.scopusqualityQ1
dc.identifier.urihttps://doi.org/10.1016/j.foodchem.2024.141098
dc.identifier.urihttps://hdl.handle.net/20.500.12418/30366
dc.identifier.volume463
dc.identifier.wosWOS:001315234600001
dc.identifier.wosqualityN/A
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.indekslendigikaynakPubMed
dc.language.isoen
dc.publisherElsevier Sci Ltd
dc.relation.ispartofFood Chemistry
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.subjectCentral composite design
dc.subjectManeb
dc.subjectDetermination
dc.subjectSample preparation
dc.subjectComplex sample matrices
dc.titleUltrasound-assisted dispersive micro solid phase extraction of maneb in water and food samples with new hybrid block copolymer material prior to micro-spectrophotometric analysis
dc.typeArticle

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