Vortex-assisted dispersive solid-phase microextraction of manganese in food samples by using newly synthesized biodegradable poly (3-hydroxy butyrate) diethanol amine

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dc.contributor.authorAltunay, Nail
dc.contributor.authorHazer, Baki
dc.contributor.authorLanjwani, Muhammad Farooque
dc.contributor.authorTuzen, Mustafa
dc.date.accessioned2024-10-26T18:09:51Z
dc.date.available2024-10-26T18:09:51Z
dc.date.issued2024
dc.departmentSivas Cumhuriyet Üniversitesi
dc.description.abstractA newly synthesized biodegradable polyhydroxy butyrate diethanol amin (PHB-DEA) was used as adsorbent for vortex assisted dispersive solid phase microextraction (VA-dSP mu E) of manganese in food samples. The different parameters were optimized such as pH, amount of adsorbent, time, desorption solvents and also number of reuses. After the sample preparation step, the determination of manganese from food samples was carried out using flame atomic absorption spectrometry. The present developed method showed good LOD value 0.15 ng mL(-1) and LOQ 0.5 ng mL(-1). The 0.5-300 ng mL(-1) linearity range was found and enhancement factor was 182. The inter-day RSD% was 2.2-4.1 and intra-day RSD% was 2.8-5.2. The recovery of manganese was found in 95-98 % . The factorial design was employed such as response surface plots, pareto chart, residual plots and ANOVA to estimate the significant level of the model using central composite design (CCD). The developed VA-dSP mu E procedure was successfully implemented to determine manganese in food samples.
dc.description.sponsorshipKapadokya University [KUN.2020-BAGP-345 001]; Turkish Academy of Sciences (TUBA), Turkey
dc.description.sponsorshipThe Kapadokya University Research Funds (#KUN.2020-BAGP-345 001) provided funding for this project. Dr. Mustafa Tuzen thanks to Turkish Academy of Sciences (TUBA) , Turkey for partial supports.
dc.identifier.doi10.1016/j.jfca.2024.106778
dc.identifier.issn0889-1575
dc.identifier.issn1096-0481
dc.identifier.scopus2-s2.0-85204742013
dc.identifier.scopusqualityQ1
dc.identifier.urihttps://doi.org/10.1016/j.jfca.2024.106778
dc.identifier.urihttps://hdl.handle.net/20.500.12418/30293
dc.identifier.volume136
dc.identifier.wosWOS:001327232900001
dc.identifier.wosqualityN/A
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoen
dc.publisherAcademic Press Inc Elsevier Science
dc.relation.ispartofJournal of Food Composition and Analysis
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.subjectFood chemistry
dc.subjectSample preparation
dc.subjectMicroextraction
dc.subjectFlame atomic absorption spectrometry
dc.subjectExperimental design
dc.subjectGreen analytical chemistry
dc.titleVortex-assisted dispersive solid-phase microextraction of manganese in food samples by using newly synthesized biodegradable poly (3-hydroxy butyrate) diethanol amine
dc.typeArticle

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